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Information card for entry 4323641
Preview
Coordinates | 4323641.cif |
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Original paper (by DOI) | HTML |
Formula | C63 H94 Au2 Cl N O4 P3 |
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Calculated formula | C63 H84 Au2 Cl N O4 P3 |
Title of publication | Restricted Rotation around the P-C Bond in Metalated Phosphonium Salts: A Variable-Temperature 1H NMR Study. X-ray Crystal Structures of [{AuP(C6H11)3}2{μ-C(PTo3)(py-2)}]ClO4 and [(AuPPh3)2{μ-{C(PPh3)(py-2)}(AuPPh3)}](CF3SO3)2 |
Authors of publication | José Vicente; María-Teresa Chicote; María-Cristina Lagunas; Peter G. Jones; Birte Ahrens |
Journal of publication | Inorganic Chemistry |
Year of publication | 1997 |
Journal volume | 36 |
Pages of publication | 4938 - 4944 |
a | 14.056 ± 0.003 Å |
b | 24.556 ± 0.004 Å |
c | 19.11 ± 0.003 Å |
α | 90° |
β | 111 ± 0.02° |
γ | 90° |
Cell volume | 6158 ± 2 Å3 |
Cell temperature | 143 ± 2 K |
Ambient diffraction temperature | 143 ± 2 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.065 |
Residual factor for significantly intense reflections | 0.0422 |
Weighted residual factors for all reflections | 0.0943 |
Weighted residual factors for significantly intense reflections | 0.0789 |
Goodness-of-fit parameter for all reflections | 1.065 |
Goodness-of-fit parameter for significantly intense reflections | 1.069 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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