Information card for entry 4323668

Structure parameters

• Formula: C37 H60 B10 O P Rh Si
• Calculated formula: C37 H52 B10 O P Rh Si
• Title of publication: Synthesis of the first Metallasila-closo-dodecaborates(1-). Silaborate Complexes of Cobalt, Rhodium, and Iridium
• Authors of publication: Lars Wesemann; Yves Ramjoie; Michael Trinkaus; Beate Ganter
• Journal of publication: Inorganic Chemistry
• Year of publication: 1997
• Journal volume: 36
• Pages of publication: 5192 - 5197
• a: 9.838 ± 0.004 Å
• b: 11.312 ± 0.003 Å
• c: 18.858 ± 0.005 Å
• α: 92.68 ± 0.02°
• β: 90.22 ± 0.03°
• γ: 96.77 ± 0.03°
• Cell volume: 2081.7 ± 1.2 ų
• Cell temperature: 203 K
• Ambient diffraction temperature: 203 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.162
• Residual factor for significantly intense reflections: 0.063
• Weighted residual factors for significantly intense reflections: 0.062
• Goodness-of-fit parameter for significantly intense reflections: 1.355
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Mo-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No