Crystallography Open Database

Information card for entry 4323704

Preview

Coordinates	4323704.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C90 H68 Ag2 Cl2 F16 O6 P6 Pd2 S4
Calculated formula	C90 H66 Ag2 Cl2 F16 O6 P6 Pd2 S4
Title of publication	Synthesis and Crystal Structure of the First Cluster Displaying PdI-AgI Interactions: [Ag2Pd2(SC6F5)2(SO3CF3)(dppm)3]SO3CF3.CH2Cl2
Authors of publication	Rafael Usón; Miguel A. Usón; Santiago Herrero
Journal of publication	Inorganic Chemistry
Year of publication	1997
Journal volume	36
Pages of publication	5959 - 5961
a	15.462 ± 0.005 Å
b	17.297 ± 0.006 Å
c	19.933 ± 0.006 Å
α	79.03 ± 0.03°
β	87.14 ± 0.02°
γ	76.44 ± 0.02°
Cell volume	5088 ± 3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	9
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0791
Residual factor for significantly intense reflections	0.0536
Weighted residual factors for all reflections	0.1454
Weighted residual factors for significantly intense reflections	0.1322
Goodness-of-fit parameter for all reflections	1.03
Goodness-of-fit parameter for significantly intense reflections	1.124
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4323704.html