Information card for entry 4323784

Structure parameters

• Formula: C24 H31 Cl N O P Pd
• Calculated formula: C24 H31 Cl N O P Pd
• Title of publication: First Resolution of a Free Fluorophosphine Chiral at Phosphorus. Resolution and Reactions of Free and Coordinated (\±)-Fluorophenylisopropylphosphine
• Authors of publication: Michael Pabel; Anthony C. Willis; S. Bruce Wild
• Journal of publication: Inorganic Chemistry
• Year of publication: 1996
• Journal volume: 35
• Pages of publication: 1244 - 1249
• a: 10.444 ± 0.003 Å
• b: 12.146 ± 0.003 Å
• c: 19.047 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2416.2 ± 1 ų
• Cell temperature: 296.2 K
• Ambient diffraction temperature: 296.2 K
• Number of distinct elements: 7
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for significantly intense reflections: 0.026
• Weighted residual factors for significantly intense reflections: 0.029
• Goodness-of-fit parameter for significantly intense reflections: 1.54
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKalpha
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No