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Information card for entry 4323820
Preview
Coordinates | 4323820.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | 1,4,8,11-tetraazacyclotetradecane-2,2'-bipyridine-ruthenium(II) bis(tetrafluoroborate) monohydrate |
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Formula | C20 H34 B2 F8 N6 O Ru |
Calculated formula | C20 H32 B2 F8 N6 O Ru |
Title of publication | Syntheses and Crystal Structures of Ruthenium Complexes of 1,4,8,11-Tetraazacyclotetradecane, Tris(2-aminoethyl)amine (tren), and Bis(2-aminoethyl)(iminomethyl)amine. A Microporous Layered Structure Consisting of {[K(tren)]2[RuCl6]}nn- and {(H5O2)4[RuCl6]}nn+ |
Authors of publication | Ken Sakai; Yasutaka Yamada; Taro Tsubomura |
Journal of publication | Inorganic Chemistry |
Year of publication | 1996 |
Journal volume | 35 |
Pages of publication | 3163 - 3172 |
a | 12.448 ± 0.003 Å |
b | 13.2 ± 0.007 Å |
c | 17.973 ± 0.004 Å |
α | 90° |
β | 104.28 ± 0.02° |
γ | 90° |
Cell volume | 2862 ± 1.8 Å3 |
Cell temperature | 296 K |
Ambient diffraction temperature | 296 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for significantly intense reflections | 0.0814 |
Weighted residual factors for significantly intense reflections | 0.0707 |
Goodness-of-fit parameter for significantly intense reflections | 4.75 |
Diffraction radiation wavelength | 0.71069 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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