Information card for entry 4323858

Structure parameters

• Formula: C47 H58 Cl2 N4 Rh4 S2
• Calculated formula: C47.5 H56 Cl2 N4 Rh4 S2
• Title of publication: Stepwise Construction of Polynuclear Complexes of Rhodium and Iridium Assisted by Benzimidazole-2-thiol. NMR and X-ray Diffraction Studies
• Authors of publication: Cristina Tejel; B. Eva Villarroya; Miguel A. Ciriano; Luis A. Oro; Maurizio Lanfranchi; Antonio Tiripicchio; Marisa Tiripicchio-Camellini
• Journal of publication: Inorganic Chemistry
• Year of publication: 1996
• Journal volume: 35
• Pages of publication: 4360 - 4368
• a: 20.173 ± 0.005 Å
• b: 42.076 ± 0.008 Å
• c: 10.983 ± 0.003 Å
• α: 90 ± 0°
• β: 93.32 ± 0.02°
• γ: 90 ± 0°
• Cell volume: 9307 ± 4 ų
• Cell temperature: 295 K
• Ambient diffraction temperature: 295 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.0622
• Weighted residual factors for significantly intense reflections: 0.0779
• Goodness-of-fit parameter for significantly intense reflections: 1.05
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: Cu-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No