Information card for entry 4323864

Structure parameters

• Common name: pentachloro-tris(1,3,6-)-trimethylphosphino-dirhenium (II, III) dichloromethane solvate
• Chemical name: pentachloro-tris(1,3,6-)-trimethylphosphino-dirhenium (II, III) dichloromethane solvate
• Formula: C9.5 H28 Cl6 P3 Re2
• Calculated formula: C9.5 H28 Cl6 P3 Re2
• Title of publication: Further Studies of the Isomeric 1,2,7- and 1,3,6-Re2Cl5(PMe3)3 Compounds
• Authors of publication: F. Albert Cotton; Evgeny V. Dikarev
• Journal of publication: Inorganic Chemistry
• Year of publication: 1996
• Journal volume: 35
• Pages of publication: 4738 - 4742
• a: 8.907 ± 0.001 Å
• b: 16.112 ± 0.001 Å
• c: 16.683 ± 0.003 Å
• α: 90°
• β: 94.751 ± 0.006°
• γ: 90°
• Cell volume: 2385.9 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0716
• Residual factor for significantly intense reflections: 0.0491
• Weighted residual factors for all reflections: 0.1476
• Weighted residual factors for significantly intense reflections: 0.1319
• Goodness-of-fit parameter for all reflections: 1.058
• Goodness-of-fit parameter for significantly intense reflections: 1.075
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No