Information card for entry 4323879

Structure parameters

• Common name: [Pd(dino[18]mac)](ClO~4~)~2~
• Chemical name: (3,12-Dimethyl-3,12-dinitro-1,5,10,14-tetraazacyclooctadecane)palladium(II) perchlorate
• Formula: C16 H32 Cl2 N6 O14 Pd
• Calculated formula: C16 H32 Cl2 N6 O14 Pd
• Title of publication: "Swollen" Macrocycles: Palladium(II)-Directed Template Syntheses of Pendant-Arm 14-, 16-, and 18-Membered Macrocycles
• Authors of publication: Monica Rossignoli; Christine C. Allen; Trevor W. Hambley; Geoffrey A. Lawrance; Marcel Maeder
• Journal of publication: Inorganic Chemistry
• Year of publication: 1996
• Journal volume: 35
• Pages of publication: 4961 - 4966
• a: 7.746 ± 0.005 Å
• b: 9.912 ± 0.005 Å
• c: 18.96 ± 0.02 Å
• α: 91.76 ± 0.06°
• β: 101.73 ± 0.07°
• γ: 112.83 ± 0.05°
• Cell volume: 1303.9 ± 1.9 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.085
• Residual factor for significantly intense reflections: 0.0713
• Weighted residual factors for all reflections: 0.2149
• Weighted residual factors for significantly intense reflections: 0.2061
• Goodness-of-fit parameter for all reflections: 1.044
• Goodness-of-fit parameter for significantly intense reflections: 1.11
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No