Information card for entry 4323968

Structure parameters

• Formula: C62 Cl3 F3 N2 O4 P4 Re2 S
• Calculated formula: C65 H59 Cl3 F3 N3 O4 P4 Re2 S
• Title of publication: Reactions of the Dirhenium(II) Complexes Re~2~X~4~(μ-dppm)~2~ (X = Cl, Br; dppm = Ph~2~PCH~2~PPh~2~) with Isocyanides. 11.1 A Triply Bonded Dirhenium Complex Containing a Labile Acetonitrile Ligand. Synthesis, Structural Characterization, and Reactivity of [(XylNC)(CH~3~CN)ClRe(μ-dppm)~2~ReCl~2~(CO)]O~3~SCF~3~
• Authors of publication: Wengan Wu; J. Anand Subramony; Phillip E. Fanwick; Richard A. Walton
• Journal of publication: Inorganic Chemistry
• Year of publication: 1996
• Journal volume: 35
• Pages of publication: 6784 - 6788
• a: 17.556 ± 0.003 Å
• b: 14.988 ± 0.003 Å
• c: 25.699 ± 0.007 Å
• α: 90°
• β: 93.98 ± 0.07°
• γ: 90°
• Cell volume: 6746 ± 3 ų
• Cell temperature: 293 K
• Ambient diffraction temperature: 293 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.136
• Residual factor for significantly intense reflections: 0.041
• Weighted residual factors for significantly intense reflections: 0.049
• Goodness-of-fit parameter for significantly intense reflections: 0.341
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Mo-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No