Information card for entry 4324018

Structure parameters

• Formula: C28 H22 N4 O4 Pd
• Calculated formula: C28 H22 N4 O4 Pd
• Title of publication: Bonding Forces in Short Hydrogen Bonds. Crystal Structure of PdII(dpgH)2
• Authors of publication: Ronald F. See; Christopher J. Curtis; Kevin W. McConnell; Seethraman Santhanam; William M. Strub; Joseph W. Ziller
• Journal of publication: Inorganic Chemistry
• Year of publication: 1997
• Journal volume: 36
• Pages of publication: 4151 - 4155
• a: 15.324 ± 0.002 Å
• b: 22.634 ± 0.003 Å
• c: 6.8811 ± 0.0007 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2386.7 ± 0.5 ų
• Cell temperature: 158 ± 2 K
• Ambient diffraction temperature: 158 ± 2 K
• Number of distinct elements: 5
• Space group number: 72
• Hermann-Mauguin space group symbol: I b a m
• Hall space group symbol: -I 2 2c
• Residual factor for all reflections: 0.079
• Residual factor for significantly intense reflections: 0.0488
• Weighted residual factors for all reflections: 0.1358
• Weighted residual factors for significantly intense reflections: 0.1267
• Goodness-of-fit parameter for all reflections: 1.29
• Goodness-of-fit parameter for significantly intense reflections: 1.423
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No