Information card for entry 4324037

Structure parameters

• Formula: C17 H30 Cl16 O8 Sb2 Ti
• Calculated formula: C17 H30 Cl16 O8 Sb2 Ti
• Title of publication: Ionization of TiCl4 and MgCl2 during the Formation of a High-Activity α-Olefin Polymerization Catalyst. Crystal Structures of [cis-{C2H4(CO2Et)2}2Cl2Ti][SbCl6]2.CH2Cl2 and [Mg{C2H4(CO2Et)2}3][MgCl4].2CH2Cl2
• Authors of publication: Piotr Sobota; Sławomir Szafert
• Journal of publication: Inorganic Chemistry
• Year of publication: 1996
• Journal volume: 35
• Pages of publication: 1778 - 1781
• a: 16.178 ± 0.005 Å
• b: 12.784 ± 0.004 Å
• c: 10.427 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2156.5 ± 1 ų
• Cell temperature: 270 ± 1 K
• Ambient diffraction temperature: 270 ± 1 K
• Number of distinct elements: 6
• Space group number: 34
• Hermann-Mauguin space group symbol: P n n 2
• Hall space group symbol: P 2 -2n
• Residual factor for significantly intense reflections: 0.0361
• Weighted residual factors for significantly intense reflections: 0.0859
• Goodness-of-fit parameter for significantly intense reflections: 1.17
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No