Information card for entry 4324059

Structure parameters

• Formula: C20 H32 I O10 P4 Re
• Calculated formula: C20 H32 I O10 P4 Re
• Title of publication: Chemistry in Environmentally Benign Media. 3.1 Synthesis and Characterization of Rhenium(V) Complexes Derived from Novel Water-Soluble (Hydroxymethyl)phosphines. Crystal Structures of [Re(O)2{(HOH2C)2PC6H4P(CH2OH)2}2]I and [Re(O)2{(HOH2C)2PCH2CH2P(CH2OH)2}2]Cl
• Authors of publication: V. Sreenivasa Reddy; Douglas E. Berning; Kattesh Katti; Charles L. Barnes; Wynn A. Volkert; A.R. Kettring
• Journal of publication: Inorganic Chemistry
• Year of publication: 1996
• Journal volume: 35
• Pages of publication: 1753 - 1757
• a: 23.906 ± 0.005 Å
• b: 7.0493 ± 0.0006 Å
• c: 17.024 ± 0.004 Å
• α: 90°
• β: 105.929 ± 0.009°
• γ: 90°
• Cell volume: 2758.7 ± 0.9 ų
• Cell temperature: 293 K
• Ambient diffraction temperature: 293 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.019
• Residual factor for significantly intense reflections: 0.019
• Weighted residual factors for all reflections: 0.027
• Weighted residual factors for significantly intense reflections: 0.027
• Goodness-of-fit parameter for significantly intense reflections: 1.21
• Diffraction radiation wavelength: 0.7093 Å
• Diffraction radiation type: MolybdenumKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No