Information card for entry 4324074

Structure parameters

• Formula: C67 H99 K N4 O9 Rh
• Calculated formula: C67 H99 K N4 O9 Rh
• Title of publication: Redox Behavior of Rhodium 9,10-Phenanthrenediimine Complexes
• Authors of publication: David W. Shaffer; Scott A. Ryken; Ryan A. Zarkesh; Alan F. Heyduk
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 13 - 21
• a: 12.5891 ± 0.0007 Å
• b: 24.1291 ± 0.0013 Å
• c: 22.6328 ± 0.0012 Å
• α: 90°
• β: 105.223 ± 0.001°
• γ: 90°
• Cell volume: 6633.8 ± 0.6 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0615
• Residual factor for significantly intense reflections: 0.0376
• Weighted residual factors for significantly intense reflections: 0.0785
• Weighted residual factors for all reflections included in the refinement: 0.0874
• Goodness-of-fit parameter for all reflections included in the refinement: 0.997
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No