Information card for entry 4324095

Structure parameters

• Formula: H282 K12 Mn14 O325 P8 W48
• Calculated formula: K10.8 Mn14 O252 P8 W48
• Title of publication: Extended Polyoxometalate Framework Solids: Two Mn(II)-Linked {P8W48} Network Arrays
• Authors of publication: Scott G. Mitchell; Thomas Boyd; Haralampos N. Miras; De-Liang Long; Leroy Cronin
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 136 - 143
• a: 45.766 ± 0.003 Å
• b: 14.3753 ± 0.0008 Å
• c: 26.618 ± 0.003 Å
• α: 90°
• β: 123.916 ± 0.005°
• γ: 90°
• Cell volume: 14532 ± 2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for all reflections: 0.16
• Residual factor for significantly intense reflections: 0.1251
• Weighted residual factors for significantly intense reflections: 0.3172
• Weighted residual factors for all reflections included in the refinement: 0.3403
• Goodness-of-fit parameter for all reflections included in the refinement: 1.16
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No