Information card for entry 4324160

Structure parameters

• Formula: C24.25 H10.5 B Cl0.5 F10 P
• Calculated formula: C24.25 H10.5 B Cl0.5 F10 P
• Title of publication: Synthesis and Reactivity of the Phosphinoboranes R2PB(C6F5)2
• Authors of publication: Stephen J. Geier; Thomas M. Gilbert; Douglas W. Stephan
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 336 - 344
• a: 10.3197 ± 0.0016 Å
• b: 12.0982 ± 0.0019 Å
• c: 20.926 ± 0.003 Å
• α: 74.492 ± 0.002°
• β: 76.7 ± 0.002°
• γ: 68.458 ± 0.002°
• Cell volume: 2316.2 ± 0.6 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1486
• Residual factor for significantly intense reflections: 0.0573
• Weighted residual factors for significantly intense reflections: 0.1054
• Weighted residual factors for all reflections included in the refinement: 0.1347
• Goodness-of-fit parameter for all reflections included in the refinement: 0.919
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No