Information card for entry 4324474

Structure parameters

• Formula: C148 H210 Fe9 N10 O8 S6 Si4
• Calculated formula: C148 H210 Fe9 N10 O8 S6 Si4
• Title of publication: Iron-Mediated Hydrazine Reduction and the Formation of Iron-Arylimide Heterocubanes
• Authors of publication: Michael J. Zdilla; Atul K. Verma; Sonny C. Lee
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 1551 - 1562
• a: 25.5272 ± 0.0005 Å
• b: 21.9314 ± 0.0005 Å
• c: 30.2981 ± 0.0006 Å
• α: 90°
• β: 113.899 ± 0.001°
• γ: 90°
• Cell volume: 15508 ± 0.6 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1151
• Residual factor for significantly intense reflections: 0.0686
• Weighted residual factors for all reflections: 0.1686
• Weighted residual factors for significantly intense reflections: 0.1466
• Goodness-of-fit parameter for all reflections: 1.033
• Goodness-of-fit parameter for significantly intense reflections: 1.123
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No