Information card for entry 4324673

Structure parameters

• Common name: complex3
• Formula: C49 H55.3 B F4.7 O P2 Rh
• Calculated formula: C49 H55.288 B F4.712 O P2 Rh
• Title of publication: Study of the Conformationally Flexible, Wide Bite-Angle Diphosphine 4,6-Bis(3-diisopropylphosphinophenyl)dibenzofuran in Rhodium(I) and Palladium(II) Coordination Complexes
• Authors of publication: Keying Ding; Deanna L. Miller; Victor G. Young; Connie C. Lu
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 2545 - 2552
• a: 12.888 ± 0.0014 Å
• b: 13.1496 ± 0.0014 Å
• c: 14.7016 ± 0.0016 Å
• α: 103.481 ± 0.002°
• β: 108.628 ± 0.002°
• γ: 104.214 ± 0.002°
• Cell volume: 2153 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0719
• Residual factor for significantly intense reflections: 0.0458
• Weighted residual factors for significantly intense reflections: 0.0984
• Weighted residual factors for all reflections included in the refinement: 0.1101
• Goodness-of-fit parameter for all reflections included in the refinement: 1.048
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No