Information card for entry 4324889

Structure parameters

• Formula: C52 H84 Cu9 N66
• Calculated formula: C52 H84 Cu9 N66.24
• Title of publication: Synthesis, Structures, and Magnetic Behavior of a Series of Copper(II) Azide Polymers of Cu4 Building Clusters and Isolation of a New Hemiaminal Ether as the Metal Complex
• Authors of publication: Sandip Mukherjee; Bappaditya Gole; You Song; Partha Sarathi Mukherjee
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 3621 - 3631
• a: 10.92 ± 0.0003 Å
• b: 11.1292 ± 0.0003 Å
• c: 20.3016 ± 0.0005 Å
• α: 91.627 ± 0.001°
• β: 90.081 ± 0.001°
• γ: 115.39 ± 0.001°
• Cell volume: 2227.81 ± 0.1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1005
• Residual factor for significantly intense reflections: 0.0444
• Weighted residual factors for significantly intense reflections: 0.0878
• Weighted residual factors for all reflections included in the refinement: 0.1031
• Goodness-of-fit parameter for all reflections included in the refinement: 0.997
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No