Information card for entry 4324897

Structure parameters

• Formula: C136 H136 Cl4 N12 Pd4
• Calculated formula: C136 H136 Cl4 N12 Pd4
• Title of publication: Synthesis and Characterization of Pd Complexes of a Carbazolyl/Bis(Imine) NNN Pincer Ligand
• Authors of publication: Aaron M. Hollas; Weixing Gu; Nattamai Bhuvanesh; Oleg V. Ozerov
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 3673 - 3679
• a: 13.7812 ± 0.0016 Å
• b: 11.62 ± 0.0013 Å
• c: 20.45 ± 0.003 Å
• α: 90°
• β: 118.777 ± 0.008°
• γ: 90°
• Cell volume: 2870.4 ± 0.7 ų
• Cell temperature: 110 ± 2 K
• Ambient diffraction temperature: 110 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0788
• Residual factor for significantly intense reflections: 0.041
• Weighted residual factors for significantly intense reflections: 0.085
• Weighted residual factors for all reflections included in the refinement: 0.094
• Goodness-of-fit parameter for all reflections included in the refinement: 0.766
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No