Information card for entry 4324990

Structure parameters

• Formula: C16 H17 Cl4 Mo N2 O2
• Calculated formula: C16 H17 Cl4 Mo N2 O2
• Title of publication: C-N Bond-Forming Self-Condensation of Amide Promoted by MoCl5 at Room Temperature
• Authors of publication: Sara Dolci; Fabio Marchetti; Guido Pampaloni; Stefano Zacchini
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 3846 - 3848
• a: 10.869 ± 0.006 Å
• b: 15.895 ± 0.008 Å
• c: 11.934 ± 0.006 Å
• α: 90°
• β: 107.727 ± 0.006°
• γ: 90°
• Cell volume: 1963.9 ± 1.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1356
• Residual factor for significantly intense reflections: 0.0708
• Weighted residual factors for significantly intense reflections: 0.1693
• Weighted residual factors for all reflections included in the refinement: 0.225
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No