Information card for entry 4325145

Structure parameters

• Common name: pentakis(triethylphosphino)-hexakis(copper-phenyltellurolate)
• Chemical name: pentakis(μ~3~-phenyltellurido)-(μ~2~-phenyltellurido) -pentakis(triethylphosphine)-hexa-copper
• Formula: C66 H105 Cu6 P5 Te6
• Calculated formula: C66 H105 Cu6 P5 Te6
• Title of publication: Trialkylphosphine-Stabilized Copper(I) Phenylchalcogenolate Complexes - Crystal Structures and Copper-Chalcogenolate Bonding
• Authors of publication: Oliver Kluge; Katharina Grummt; Ralf Biedermann; Harald Krautscheid
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 4742 - 4752
• a: 21.6472 ± 0.0006 Å
• b: 15.5979 ± 0.0005 Å
• c: 24.1542 ± 0.0007 Å
• α: 90°
• β: 98.176 ± 0.002°
• γ: 90°
• Cell volume: 8072.8 ± 0.4 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0416
• Residual factor for significantly intense reflections: 0.0306
• Weighted residual factors for significantly intense reflections: 0.073
• Weighted residual factors for all reflections included in the refinement: 0.0763
• Goodness-of-fit parameter for all reflections included in the refinement: 0.985
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No