Information card for entry 4325195

Structure parameters

• Formula: C Cl Cs2.5 Dy3 Na4 O97.5 Si2 W18
• Calculated formula: C Cl Cs2.5 Dy3 Na4 O97.5 Si2 W18
• Title of publication: Lanthanoid-Containing Open Wells-Dawson Silicotungstates: Synthesis, Crystal Structures, and Properties
• Authors of publication: Lubin Ni; Firasat Hussain; Bernhard Spingler; Stephen Weyeneth; Greta R. Patzke
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 4944 - 4955
• a: 12.8335 ± 0.0003 Å
• b: 15.7343 ± 0.0003 Å
• c: 23.1443 ± 0.0004 Å
• α: 99.304 ± 0.002°
• β: 98.206 ± 0.002°
• γ: 92.871 ± 0.002°
• Cell volume: 4551.91 ± 0.16 ų
• Cell temperature: 183 ± 2 K
• Ambient diffraction temperature: 183 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0705
• Residual factor for significantly intense reflections: 0.0401
• Weighted residual factors for significantly intense reflections: 0.0837
• Weighted residual factors for all reflections included in the refinement: 0.0884
• Goodness-of-fit parameter for all reflections included in the refinement: 0.921
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No