Information card for entry 4325300

Structure parameters

• Formula: C13 H20 Cl2 N2 Ru
• Calculated formula: C13 H20 Cl2 N2 Ru
• Title of publication: Synthesis and Structure of Ruthenium(IV) Complexes Featuring N-Heterocyclic Ligands with an N-H Group as the Hydrogen-Bond Donor: Hydrogen Interactions in Solution and in the Solid State
• Authors of publication: Josefina Díez; José Gimeno; Isabel Merino; Eduardo Rubio; Francisco J. Suárez
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 4868 - 4881
• a: 33.2559 ± 0.0008 Å
• b: 24.4116 ± 0.0006 Å
• c: 11.1014 ± 0.0002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 9012.4 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 43
• Hermann-Mauguin space group symbol: F d d 2
• Hall space group symbol: F 2 -2d
• Residual factor for all reflections: 0.0443
• Residual factor for significantly intense reflections: 0.0426
• Weighted residual factors for significantly intense reflections: 0.115
• Weighted residual factors for all reflections included in the refinement: 0.1166
• Goodness-of-fit parameter for all reflections included in the refinement: 1.073
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No