Information card for entry 4325357

Structure parameters

• Chemical name: U(V)(OSiPh3)(OBCF)(AcNac)2
• Formula: C125.5 H115 B F15 N2 O4 Si U
• Calculated formula: C125.5 H79 B F15 N2 O4 Si U
• Title of publication: Borane-Mediated Silylation of a Metal-Oxo Ligand
• Authors of publication: David D. Schnaars; Guang Wu; Trevor W. Hayton
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 4695 - 4697
• a: 17.5521 ± 0.0019 Å
• b: 19.1663 ± 0.0019 Å
• c: 32.687 ± 0.004 Å
• α: 90°
• β: 98.161 ± 0.004°
• γ: 90°
• Cell volume: 10885 ± 2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.2012
• Residual factor for significantly intense reflections: 0.1051
• Weighted residual factors for significantly intense reflections: 0.219
• Weighted residual factors for all reflections included in the refinement: 0.2702
• Goodness-of-fit parameter for all reflections included in the refinement: 1.007
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No