Information card for entry 4325362

Structure parameters

• Formula: C49 H64 O P2 Rh2 n4
• Calculated formula: C49 H64 N4 O P2 Rh2
• Title of publication: Comparison of Structure and Reactivity of Phosphine-Amido and Hemilabile Phosphine-Amine Chelates of Rhodium
• Authors of publication: Lindsay J. Hounjet; Robert McDonald; Michael J. Ferguson; Martin Cowie
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 5361 - 5378
• a: 15.1371 ± 0.0017 Å
• b: 11.9719 ± 0.0014 Å
• c: 12.1833 ± 0.0014 Å
• α: 90°
• β: 96.598 ± 0.001°
• γ: 90°
• Cell volume: 2193.2 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 5
• Hermann-Mauguin space group symbol: C 1 2 1
• Hall space group symbol: C 2y
• Residual factor for all reflections: 0.0279
• Residual factor for significantly intense reflections: 0.0275
• Weighted residual factors for significantly intense reflections: 0.0669
• Weighted residual factors for all reflections included in the refinement: 0.067
• Goodness-of-fit parameter for all reflections included in the refinement: 1.212
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No