Information card for entry 4325367

Structure parameters

• Formula: C28 H30 F3 O3 P Rh S n
• Calculated formula: C28 H30 F3 N O3 P Rh S
• Title of publication: Comparison of Structure and Reactivity of Phosphine-Amido and Hemilabile Phosphine-Amine Chelates of Rhodium
• Authors of publication: Lindsay J. Hounjet; Robert McDonald; Michael J. Ferguson; Martin Cowie
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 5361 - 5378
• a: 10.0204 ± 0.0005 Å
• b: 13.4944 ± 0.0007 Å
• c: 21.7084 ± 0.0011 Å
• α: 105.821 ± 0.0006°
• β: 90.9298 ± 0.0006°
• γ: 103.704 ± 0.0006°
• Cell volume: 2733.5 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0456
• Residual factor for significantly intense reflections: 0.0396
• Weighted residual factors for significantly intense reflections: 0.0888
• Weighted residual factors for all reflections included in the refinement: 0.0918
• Goodness-of-fit parameter for all reflections included in the refinement: 1.088
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No