Information card for entry 4325396

Structure parameters

• Common name: [(C66H72N6O12)Zn6(EtCO2)5(OH)(H2O)]2_(CH2Cl2)2(MeOH)2(H2O)2(C6H14)
• Formula: C172 H230 Cl4 O52 Zn12 n12
• Calculated formula: C172 H230 Cl4 N12 O52 Zn12
• Title of publication: Nuclearity Control of a Trisaloph Zinc Cluster Complex Dependent on Minute Structural Differences in the Bridging Anions
• Authors of publication: Masaki Yamamura; Hayato Miyazaki; Masaya Iida; Shigehisa Akine; Tatsuya Nabeshima
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 5315 - 5317
• a: 15.288 ± 0.006 Å
• b: 17.956 ± 0.006 Å
• c: 18.488 ± 0.005 Å
• α: 68.243 ± 0.011°
• β: 76.237 ± 0.012°
• γ: 80.298 ± 0.014°
• Cell volume: 4560 ± 3 ų
• Cell temperature: 120 K
• Ambient diffraction temperature: 120 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1662
• Residual factor for significantly intense reflections: 0.0921
• Weighted residual factors for significantly intense reflections: 0.2042
• Weighted residual factors for all reflections included in the refinement: 0.2443
• Goodness-of-fit parameter for all reflections included in the refinement: 1.099
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No