Information card for entry 4325563

Structure parameters

• Formula: C54 H45 Cl8 P3 Pd2 S2
• Calculated formula: C54 H45 Cl8 P3 Pd2 S2
• Title of publication: 1,3-Bis(thiophosphinoyl)indene: A Unique and Versatile Scaffold for Original Polymetallic Complexes
• Authors of publication: Noel Nebra; Nathalie Saffon; Laurent Maron; Blanca Martin-Vaca; Didier Bourissou
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 6378 - 6383
• a: 18.7145 ± 0.0004 Å
• b: 14.7029 ± 0.0003 Å
• c: 21.688 ± 0.0005 Å
• α: 90°
• β: 113.987 ± 0.001°
• γ: 90°
• Cell volume: 5452.2 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0494
• Residual factor for significantly intense reflections: 0.0265
• Weighted residual factors for significantly intense reflections: 0.0547
• Weighted residual factors for all reflections included in the refinement: 0.0661
• Goodness-of-fit parameter for all reflections included in the refinement: 1.101
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No