Information card for entry 4325565

Structure parameters

• Formula: C72 H60 Cl14 P4 Pd3 S4
• Calculated formula: C72 H60 Cl14 P4 Pd3 S4
• Title of publication: 1,3-Bis(thiophosphinoyl)indene: A Unique and Versatile Scaffold for Original Polymetallic Complexes
• Authors of publication: Noel Nebra; Nathalie Saffon; Laurent Maron; Blanca Martin-Vaca; Didier Bourissou
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 6378 - 6383
• a: 34.423 ± 0.007 Å
• b: 14.298 ± 0.003 Å
• c: 22.074 ± 0.004 Å
• α: 90°
• β: 129.45 ± 0.03°
• γ: 90°
• Cell volume: 8389 ± 5 ų
• Cell temperature: 233 ± 2 K
• Ambient diffraction temperature: 233 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.2415
• Residual factor for significantly intense reflections: 0.069
• Weighted residual factors for significantly intense reflections: 0.1205
• Weighted residual factors for all reflections included in the refinement: 0.1733
• Goodness-of-fit parameter for all reflections included in the refinement: 0.813
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No