Information card for entry 4325575

Structure parameters

• Formula: As4 H114 Mn3 Na16 O169 W30
• Calculated formula: As4 Mn3 Na16 O169 W30
• Title of publication: Manganese(III)-Containing Wells-Dawson Sandwich-Type Polyoxometalates: Comparison with their Manganese(II) Counterparts
• Authors of publication: Mounim Lebrini; Israël M. Mbomekallé; Anne Dolbecq; Jérôme Marrot; Patrick Berthet; Joseline Ntienoue; Francis Sécheresse; Jacky Vigneron; Arnaud Etcheberry
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 6437 - 6448
• a: 17.143 ± 0.003 Å
• b: 15.096 ± 0.003 Å
• c: 31.48 ± 0.006 Å
• α: 90°
• β: 90.413 ± 0.01°
• γ: 90°
• Cell volume: 8147 ± 3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0843
• Residual factor for significantly intense reflections: 0.0675
• Weighted residual factors for significantly intense reflections: 0.1868
• Weighted residual factors for all reflections included in the refinement: 0.2094
• Goodness-of-fit parameter for all reflections included in the refinement: 1.107
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No