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Information card for entry 4325819
Preview
Coordinates | 4325819.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C54 H66 Cl2 N6 Ni7 O26 |
---|---|
Calculated formula | C54 H66 Cl2 N6 Ni7 O26 |
SMILES | c12c3cccc1CN[Ni]1456[O]2[Ni]278([O]9c%10c(cccc%10C=[NH]7)[O](C)[Ni]7%10%119[O]2(C)[Ni]29%12([O]5(C)[Ni]5%13%14([O]1c1c(cccc1C=[NH]5)[O]4C)[O]1c4c(cccc4CN[Ni]451([O]1[Ni]%15([NH]=Cc%16c1c(ccc%16)[O]4C)([O]%11c1c(cccc1CN%10)[O]%15C)([O]25C)[O]7%12C)[O]9%13C)[O]%14C)[O]68C)[O]3C.[O-]Cl(=O)(=O)=O.[O-]Cl(=O)(=O)=O |
Title of publication | Microwave versus Traditional Solvothermal Synthesis of Ni7II Discs: Effect of Ligand on Exchange Reaction in Solution Studied by Electrospray Ionization-Mass Spectroscopy and Magnetic Properties |
Authors of publication | Lian-Qiang Wei; Kun Zhang; Ying-Chun Feng; Yun-Hong Wang; Ming-Hua Zeng; Mohamedally Kurmoo |
Journal of publication | Inorganic Chemistry |
Year of publication | 2011 |
Journal volume | 50 |
Pages of publication | 7274 - 7283 |
a | 14.043 ± 0.002 Å |
b | 14.043 ± 0.002 Å |
c | 9.478 ± 0.0019 Å |
α | 90° |
β | 90° |
γ | 120° |
Cell volume | 1618.7 ± 0.5 Å3 |
Cell temperature | 298 ± 2 K |
Ambient diffraction temperature | 298 ± 2 K |
Number of distinct elements | 6 |
Space group number | 147 |
Hermann-Mauguin space group symbol | P -3 |
Hall space group symbol | -P 3 |
Residual factor for all reflections | 0.1212 |
Residual factor for significantly intense reflections | 0.0627 |
Weighted residual factors for significantly intense reflections | 0.1588 |
Weighted residual factors for all reflections included in the refinement | 0.2237 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.107 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4325819.html
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Users of the data should acknowledge the original authors of the
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