Information card for entry 4325825

Structure parameters

• Chemical name: Bis(1,1,1,5,5,5-hexafluoropentane-2,2,4,4-tetraolate)- tetralead(II), chlorobenzene adduct
• Formula: C13 H6.5 Cl0.5 F12 O8 Pb4
• Calculated formula: C13 H6.5 Cl0.5 F12 O8 Pb4
• Title of publication: Homoleptic Tetranuclear Complexes of Divalent Tin and Lead Tetraolates
• Authors of publication: Zheng Wei; Jen-Hsien Yang; Volodimir D. Vreshch; Alexander V. Zabula; Alexander S. Filatov; Evgeny V. Dikarev
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 7295 - 7300
• a: 10.8813 ± 0.0006 Å
• b: 27.3449 ± 0.0016 Å
• c: 15.7652 ± 0.0009 Å
• α: 90°
• β: 93.387 ± 0.001°
• γ: 90°
• Cell volume: 4682.7 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0396
• Residual factor for significantly intense reflections: 0.0299
• Weighted residual factors for significantly intense reflections: 0.067
• Weighted residual factors for all reflections included in the refinement: 0.0706
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Mo-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No