Information card for entry 4325955

Structure parameters

• Formula: C6 H14 Co4.75 K2.5 N2 O55 Si W9
• Calculated formula: C6 H14 Co4.75 K2.5 N2 O55.03 Si W9
• Title of publication: Route for the Elaboration of Functionalized Hybrid 3d-Substituted Trivacant Keggin Anions
• Authors of publication: Guillaume Rousseau; Olivier Oms; Anne Dolbecq; Jérôme Marrot; Pierre Mialane
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 7376 - 7378
• a: 13.9971 ± 0.0017 Å
• b: 14.5785 ± 0.0018 Å
• c: 14.7621 ± 0.0019 Å
• α: 97.325 ± 0.005°
• β: 98.477 ± 0.005°
• γ: 100.96 ± 0.005°
• Cell volume: 2887.3 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0549
• Residual factor for significantly intense reflections: 0.0458
• Weighted residual factors for significantly intense reflections: 0.1215
• Weighted residual factors for all reflections included in the refinement: 0.1418
• Goodness-of-fit parameter for all reflections included in the refinement: 1.215
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No