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Information card for entry 4325998
Preview
Coordinates | 4325998.cif |
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Original paper (by DOI) | HTML |
Formula | C20 H35 Cl2 Cu N7 O8 |
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Calculated formula | C20 H35 Cl2 Cu N7 O8 |
Title of publication | Reactivity of Nickel(II) and Copper(II) Complexes of a β-Aminohydrazone Ligand with Pyridine-2-aldehyde: Macrocyclization vs Unprecedented Pyrazole Ring Synthesis via C-C Bond-Forming Reaction |
Authors of publication | Oindrila Das; Ennio Zangrando; Tapan Kanti Paine |
Journal of publication | Inorganic Chemistry |
Year of publication | 2011 |
Journal volume | 50 |
Pages of publication | 8012 - 8019 |
a | 9.72 ± 0.003 Å |
b | 16.343 ± 0.006 Å |
c | 18.657 ± 0.006 Å |
α | 71.354 ± 0.008° |
β | 79.046 ± 0.009° |
γ | 79.586 ± 0.009° |
Cell volume | 2734 ± 1.6 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1131 |
Residual factor for significantly intense reflections | 0.0777 |
Weighted residual factors for significantly intense reflections | 0.2027 |
Weighted residual factors for all reflections included in the refinement | 0.24 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.027 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4325998.html
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