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Information card for entry 4326012
Preview
Coordinates | 4326012.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C11 H28 Cl2 O0 P4 Pd2 S2 |
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Calculated formula | C11 H28 Cl2 P4 Pd2 S2 |
SMILES | C1[P](C)(C)[Pd]2([P](C[P](C)(C)[Pd](C(=S)S2)([P]1(C)C)Cl)(C)C)Cl |
Title of publication | Reactions of the Bis(dialkylphosphino)methane Complexes Pd2X2(μ-R2PCH2PR2)2 (X = halogen, R = Me or Et) with H2S, S8, COS, and CS2; Detection of Reaction Intermediates |
Authors of publication | Craig B. Pamplin; Steven J. Rettig; Brian O. Patrick; Brian R. James |
Journal of publication | Inorganic Chemistry |
Year of publication | 2011 |
Journal volume | 50 |
Pages of publication | 8094 - 8105 |
a | 27.7975 ± 0.0004 Å |
b | 27.7975 ± 0.0004 Å |
c | 17.7113 ± 0.0005 Å |
α | 90° |
β | 90° |
γ | 120° |
Cell volume | 11852 ± 0.4 Å3 |
Cell temperature | 180 ± 2 K |
Ambient diffraction temperature | 180 ± 2 K |
Number of distinct elements | 7 |
Space group number | 148 |
Hermann-Mauguin space group symbol | R -3 :H |
Hall space group symbol | -R 3 |
Residual factor for all reflections | 0.0376 |
Residual factor for significantly intense reflections | 0.0274 |
Weighted residual factors for significantly intense reflections | 0.0738 |
Weighted residual factors for all reflections included in the refinement | 0.075 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.119 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4326012.html
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