Information card for entry 4326127

Structure parameters

• Formula: C42 H49 Cl2 N2 O3 Si V
• Calculated formula: C42 H49 Cl2 N2 O3 Si V
• Title of publication: N-Heterocyclic Carbene Stabilized Dichlorosilylene Transition-Metal Complexes of V(I), Co(I), and Fe(0)
• Authors of publication: Rajendra S. Ghadwal; Ramachandran Azhakar; Kevin Pröpper; Julian J. Holstein; Birger Dittrich; Herbert W. Roesky
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 8502 - 8508
• a: 10.2337 ± 0.0002 Å
• b: 19.3235 ± 0.0003 Å
• c: 20.225 ± 0.0004 Å
• α: 90°
• β: 92.792 ± 0.001°
• γ: 90°
• Cell volume: 3994.76 ± 0.13 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.056
• Residual factor for significantly intense reflections: 0.041
• Weighted residual factors for all reflections included in the refinement: 0.056
• Goodness-of-fit parameter for all reflections included in the refinement: 4.171
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No