Information card for entry 4326379

Structure parameters

• Formula: C2 H45 Ce Cs3 Cu3 Ge2 K4 Na4 O91 W18
• Calculated formula: C2 H3 Ce Cs2.4995 Cu3 Ge2 K Na2.85 O89 W18
• Title of publication: New Type of Heterometallic 3d-4f Rhomblike Core in Weakley-Like Polyoxometalates
• Authors of publication: Santiago Reinoso; José Ramón Galán-Mascarós; Luis Lezama
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 9587 - 9593
• a: 12.5496 ± 0.0002 Å
• b: 17.4025 ± 0.0004 Å
• c: 23.317 ± 0.0005 Å
• α: 101.966 ± 0.002°
• β: 91.712 ± 0.002°
• γ: 108.183 ± 0.002°
• Cell volume: 4708.32 ± 0.18 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 10
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0668
• Residual factor for significantly intense reflections: 0.0462
• Weighted residual factors for significantly intense reflections: 0.133
• Weighted residual factors for all reflections included in the refinement: 0.1381
• Goodness-of-fit parameter for all reflections included in the refinement: 1.071
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No