Information card for entry 4326461

Structure parameters

• Formula: C84.5 H116 Cl7.5 N8 O30 V4 W4
• Calculated formula: C84.5 H116 Cl7.5 N8 O30 V4 W4
• Title of publication: Novel Heterotetranuclear V2Mo2 or V2W2 Complexes with 4,4'-Di-tert-butyl-2,2'-bipyridine: Syntheses, Crystal Structures, and Catalytic Activities
• Authors of publication: Shintaro Kodama; Akihiro Nomoto; Shigenobu Yano; Michio Ueshima; Akiya Ogawa
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 9942 - 9947
• a: 10.1338 ± 0.0003 Å
• b: 15.6779 ± 0.0005 Å
• c: 19.752 ± 0.0006 Å
• α: 72.9803 ± 0.0009°
• β: 80.3509 ± 0.0009°
• γ: 88.1885 ± 0.0009°
• Cell volume: 2957.74 ± 0.16 ų
• Cell temperature: 113.1 K
• Ambient diffraction temperature: 113.1 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0335
• Weighted residual factors for all reflections included in the refinement: 0.096
• Goodness-of-fit parameter for all reflections included in the refinement: 1.051
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No