Information card for entry 4326524

Structure parameters

• Formula: C16 H83.25 Ge20 N16 Ni3 O52.63
• Calculated formula: C16 H84.452 Ge20 N16 Ni3 O52.616
• Title of publication: Two Open-Framework Germanates with Nickel Complexes Incorporated into the Framework
• Authors of publication: Shiliang Huang; Kirsten Christensen; Maxim V. Peskov; Sihai Yang; Kuo Li; Xiaodong Zou; Junliang Sun
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 9921 - 9923
• a: 10.5529 ± 0.0003 Å
• b: 31.5559 ± 0.0005 Å
• c: 20.7333 ± 0.0002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6904.3 ± 0.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 60
• Hermann-Mauguin space group symbol: P c a n
• Hall space group symbol: -P 2n 2c
• Residual factor for all reflections: 0.0469
• Residual factor for significantly intense reflections: 0.0331
• Weighted residual factors for significantly intense reflections: 0.0746
• Weighted residual factors for all reflections included in the refinement: 0.0802
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.6889 Å
• Diffraction radiation type: Synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No