Information card for entry 4326526

Structure parameters

• Formula: C9 H24 F3 N O4 P2 S Si
• Calculated formula: C9 H24 F3 N O4 P2 S Si
• SMILES: P(=N[P+](C)(C)C)(O[Si](C)(C)C)(C)C.S(=O)(=O)(C(F)(F)F)[O-]
• Title of publication: Reactions of Phosphine Oxides with Bromophosphoranimines; Synthesis and Unusual Rearrangements of O-Donor Stabilized Phosphoranimine Cations
• Authors of publication: Martin Bendle; Keith Huynh; Mairi F. Haddow; Ian Manners
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 10292 - 10302
• a: 8.3809 ± 0.0003 Å
• b: 8.781 ± 0.0004 Å
• c: 13.91 ± 0.0006 Å
• α: 73.781 ± 0.002°
• β: 76.827 ± 0.002°
• γ: 76.643 ± 0.002°
• Cell volume: 941.61 ± 0.07 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0481
• Residual factor for significantly intense reflections: 0.0421
• Weighted residual factors for significantly intense reflections: 0.1036
• Weighted residual factors for all reflections included in the refinement: 0.1074
• Goodness-of-fit parameter for all reflections included in the refinement: 1.073
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No