Information card for entry 4326530

Structure parameters

• Formula: C20 H40 F9 N O6 P2 S Si
• Calculated formula: C20 H40 F9 N O6 P2 S Si
• Title of publication: Reactions of Phosphine Oxides with Bromophosphoranimines; Synthesis and Unusual Rearrangements of O-Donor Stabilized Phosphoranimine Cations
• Authors of publication: Martin Bendle; Keith Huynh; Mairi F. Haddow; Ian Manners
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 10292 - 10302
• a: 24.951 ± 0.0012 Å
• b: 17.4531 ± 0.0008 Å
• c: 22.1048 ± 0.0009 Å
• α: 90°
• β: 93.28 ± 0.002°
• γ: 90°
• Cell volume: 9610.3 ± 0.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1888
• Residual factor for significantly intense reflections: 0.1028
• Weighted residual factors for significantly intense reflections: 0.2156
• Weighted residual factors for all reflections included in the refinement: 0.254
• Goodness-of-fit parameter for all reflections included in the refinement: 1.077
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No