Information card for entry 4326549

Structure parameters

• Formula: H75 K9 O115 P2 Pd2 W22
• Calculated formula: K8.63 O98 P2 Pd2 W22
• Title of publication: Noble Metals in Polyoxometalate Chemistry: Palladium-Containing Derivatives of the Monolacunary Keggin and Wells-Dawson Tungstophosphates
• Authors of publication: Natalya V. Izarova; Abhishek Banerjee; Ulrich Kortz
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 10379 - 10386
• a: 22.415 ± 0.003 Å
• b: 23.941 ± 0.003 Å
• c: 22.243 ± 0.003 Å
• α: 90°
• β: 118.676 ± 0.006°
• γ: 90°
• Cell volume: 10472 ± 2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1654
• Residual factor for significantly intense reflections: 0.0836
• Weighted residual factors for significantly intense reflections: 0.1978
• Weighted residual factors for all reflections included in the refinement: 0.2524
• Goodness-of-fit parameter for all reflections included in the refinement: 1.02
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No