Information card for entry 4326552

Structure parameters

• Formula: H41 K10 O157 P4 Pd2 W34
• Calculated formula: K10.01 O138 P4 Pd2 W34
• Title of publication: Noble Metals in Polyoxometalate Chemistry: Palladium-Containing Derivatives of the Monolacunary Keggin and Wells-Dawson Tungstophosphates
• Authors of publication: Natalya V. Izarova; Abhishek Banerjee; Ulrich Kortz
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 10379 - 10386
• a: 14.6541 ± 0.0013 Å
• b: 21.595 ± 0.002 Å
• c: 26.39 ± 0.003 Å
• α: 111.025 ± 0.007°
• β: 90.772 ± 0.006°
• γ: 92.883 ± 0.006°
• Cell volume: 7780.9 ± 1.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1333
• Residual factor for significantly intense reflections: 0.0819
• Weighted residual factors for significantly intense reflections: 0.2272
• Weighted residual factors for all reflections included in the refinement: 0.287
• Goodness-of-fit parameter for all reflections included in the refinement: 1.07
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No