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Information card for entry 4326573
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Coordinates | 4326573.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | W(CO)2(O2CMe)2(CNArDipp2)2 |
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Formula | C68 H80 N2 O6 W |
Calculated formula | C68 H80 N2 O6 W |
Title of publication | Oxidative Decarbonylation of m-Terphenyl Isocyanide Complexes of Molybdenum and Tungsten: Precursors to Low-Coordinate Isocyanide Complexes |
Authors of publication | Treffly B. Ditri; Curtis E. Moore; Arnold L. Rheingold; Joshua S. Figueroa |
Journal of publication | Inorganic Chemistry |
Year of publication | 2011 |
Journal volume | 50 |
Pages of publication | 10448 - 10459 |
a | 12.7672 ± 0.0009 Å |
b | 18.9332 ± 0.0014 Å |
c | 26.1549 ± 0.0019 Å |
α | 94.569 ± 0.001° |
β | 90.21 ± 0.001° |
γ | 101.274 ± 0.001° |
Cell volume | 6179.4 ± 0.8 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0717 |
Residual factor for significantly intense reflections | 0.037 |
Weighted residual factors for significantly intense reflections | 0.0773 |
Weighted residual factors for all reflections included in the refinement | 0.0923 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.004 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4326573.html
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