Crystallography Open Database

Information card for entry 4326583

Preview

Coordinates	4326583.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C25 H23 F6 N3 O6 P Re
Calculated formula	C25 H23 F6 N3 O6 P Re
Title of publication	Observation of Inductive Effects That Cause a Change in the Rate-Determining Step for the Conversion of Rhenium Azides to Imido Complexes
Authors of publication	Nicholas E. Travia; Zhenggang Xu; Jason M. Keith; Elon A. Ison; Phillip E. Fanwick; Michael B. Hall; Mahdi M. Abu-Omar
Journal of publication	Inorganic Chemistry
Year of publication	2011
Journal volume	50
Pages of publication	10505 - 10514
a	6.8991 ± 0.0003 Å
b	13.1725 ± 0.0009 Å
c	15.8952 ± 0.0012 Å
α	95.522 ± 0.003°
β	91.505 ± 0.004°
γ	102.398 ± 0.004°
Cell volume	1402.66 ± 0.16 Å³
Cell temperature	150 K
Ambient diffraction temperature	150 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.062
Residual factor for significantly intense reflections	0.048
Weighted residual factors for significantly intense reflections	0.117
Weighted residual factors for all reflections included in the refinement	0.125
Goodness-of-fit parameter for all reflections included in the refinement	1.07
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MO-Kα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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