Information card for entry 4326757

Structure parameters

• Formula: C30 H43 K O6 Si2
• Calculated formula: C30 H43 K O6 Si2
• SMILES: [K]12345[O]6CC[O]1CC[O]2CC[O]3CC[O]4CC[O]5CC6.[SiH3-].[SiH](c1ccccc1)(c1ccccc1)c1ccccc1
• Title of publication: Structure and Bonding of KSiH3 and Its 18-Crown-6 Derivatives: Unusual Ambidentate Behavior of the SiH3- Anion
• Authors of publication: David J. Wolstenholme; Paul D. Prince; G. Sean McGrady; Michael J. Landry; Jonathan W. Steed
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 11222 - 11227
• a: 9.4687 ± 0.001 Å
• b: 9.4687 ± 0.001 Å
• c: 9.4687 ± 0.001 Å
• α: 98.201 ± 0.01°
• β: 98.201 ± 0.01°
• γ: 98.201 ± 0.01°
• Cell volume: 820.06 ± 0.16 ų
• Cell temperature: 115 ± 2 K
• Ambient diffraction temperature: 115 ± 2 K
• Number of distinct elements: 5
• Space group number: 160
• Hermann-Mauguin space group symbol: R 3 m :R
• Hall space group symbol: P 3* -2
• Residual factor for all reflections: 0.0493
• Residual factor for significantly intense reflections: 0.0378
• Weighted residual factors for significantly intense reflections: 0.0935
• Weighted residual factors for all reflections included in the refinement: 0.0966
• Goodness-of-fit parameter for all reflections included in the refinement: 1.093
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No