Information card for entry 4326847

Structure parameters

• Formula: C25 H22 Br4 P
• Calculated formula: C25 H22 Br4 P
• Title of publication: [(Ph)3PBr][Br7], [(Bz)(Ph)3P]2[Br8], [(n-Bu)3MeN]2[Br20], [C4MPyr]2[Br20], and [(Ph)3PCl]2[Cl2I14]: Extending the Horizon of Polyhalides via Synthesis in Ionic Liquids
• Authors of publication: Michael Wolff; Alexander Okrut; Claus Feldmann
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 11683 - 11694
• a: 9.045 ± 0.0018 Å
• b: 9.643 ± 0.0019 Å
• c: 14.348 ± 0.003 Å
• α: 103.77 ± 0.03°
• β: 93.72 ± 0.03°
• γ: 93.73 ± 0.03°
• Cell volume: 1208.7 ± 0.5 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.05
• Residual factor for significantly intense reflections: 0.0367
• Weighted residual factors for significantly intense reflections: 0.0923
• Weighted residual factors for all reflections included in the refinement: 0.0984
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No