Information card for entry 4326851

Structure parameters

• Formula: C9 H20 Br10 N
• Calculated formula: C9 H20 Br10 N
• Title of publication: [(Ph)3PBr][Br7], [(Bz)(Ph)3P]2[Br8], [(n-Bu)3MeN]2[Br20], [C4MPyr]2[Br20], and [(Ph)3PCl]2[Cl2I14]: Extending the Horizon of Polyhalides via Synthesis in Ionic Liquids
• Authors of publication: Michael Wolff; Alexander Okrut; Claus Feldmann
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 11683 - 11694
• a: 8.475 ± 0.0017 Å
• b: 10.996 ± 0.002 Å
• c: 13.138 ± 0.003 Å
• α: 88.77 ± 0.03°
• β: 80.12 ± 0.03°
• γ: 75.85 ± 0.02°
• Cell volume: 1169.3 ± 0.4 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 203 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0807
• Residual factor for significantly intense reflections: 0.0434
• Weighted residual factors for significantly intense reflections: 0.0969
• Weighted residual factors for all reflections included in the refinement: 0.1113
• Goodness-of-fit parameter for all reflections included in the refinement: 0.918
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No