Information card for entry 4326900

Structure parameters

• Chemical name: (K-18c6)3(KSn9)(C6H6)3
• Formula: C54 H90 K4 Ni0.6 O18 Sn9
• Calculated formula: C54 H90 K4 Ni0.602 O18 Sn9
• Title of publication: Metal-Centered Deltahedral Zintl Ions: Synthesis of [Ni@Sn9]4- by direct Extraction from Intermetallic Precursors and of the Vertex-Fused Dimer [{Ni@Sn8(μ-Ge)1/2}2]4-
• Authors of publication: Miriam M. Gillett-Kunnath; Joseph I. Paik; Sara M. Jensen; Jacob D. Taylor; Slavi C. Sevov
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 11695 - 11701
• a: 10.2754 ± 0.0005 Å
• b: 19.5442 ± 0.0009 Å
• c: 20.5576 ± 0.0013 Å
• α: 73.927 ± 0.003°
• β: 79.838 ± 0.004°
• γ: 84.389 ± 0.003°
• Cell volume: 3899.6 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0401
• Residual factor for significantly intense reflections: 0.0266
• Weighted residual factors for significantly intense reflections: 0.0658
• Weighted residual factors for all reflections included in the refinement: 0.083
• Goodness-of-fit parameter for all reflections included in the refinement: 1.151
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No