Crystallography Open Database

Information card for entry 4326954

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Coordinates	4326954.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C20 H44 B2 Co F8 N4 P4
Calculated formula	C20 H44 B2 Co F8 N4 P4
Title of publication	Synthesis and Hydride Transfer Reactions of Cobalt and Nickel Hydride Complexes to BX3 Compounds
Authors of publication	Michael T. Mock; Robert G. Potter; Molly J. O'Hagan; Donald M. Camaioni; William G. Dougherty; W. Scott Kassel; Daniel L. DuBois
Journal of publication	Inorganic Chemistry
Year of publication	2011
Journal volume	50
Pages of publication	11914 - 11928
a	8.4911 ± 0.0005 Å
b	12.9468 ± 0.0008 Å
c	15.018 ± 0.0009 Å
α	91.137 ± 0.004°
β	92.512 ± 0.004°
γ	97.786 ± 0.004°
Cell volume	1633.62 ± 0.17 Å³
Cell temperature	117 ± 2 K
Ambient diffraction temperature	117 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1121
Residual factor for significantly intense reflections	0.0537
Weighted residual factors for significantly intense reflections	0.1365
Weighted residual factors for all reflections included in the refinement	0.1656
Goodness-of-fit parameter for all reflections included in the refinement	1.011
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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